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Home > Products >  (-)-Syringaresnol-4-O-beta-D-apiofuranosyl-(1->2)-beta-D-glucopyranoside

(-)-Syringaresnol-4-O-beta-D-apiofuranosyl-(1->2)-beta-D-glucopyranoside CAS NO.136997-64-3

  • Min.Order: 10 Milligram
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Keywords

  • (-)-Syringaresnol-4-O-beta-D-apiofuranosyl-(1->2)-beta-D-glucopyranoside
  • 136997-64-3
  • standard supplier in China

Quick Details

  • ProName: (-)-Syringaresnol-4-O-beta-D-apiofuran...
  • CasNo: 136997-64-3
  • Molecular Formula: C33H44O17= C33H44O17
  • Appearance: detailed see specifications
  • Application: analysis,activity test,Botanical Refer...
  • DeliveryTime: 1-3?working?days?after?confirming?the?...
  • PackAge: According to the clients requirement.
  • Port: China main port
  • ProductionCapacity: 1 Metric Ton/Day
  • Purity: ≥98%
  • Storage: Store at 2~8°C
  • Transportation: by air or by ocean shipping
  • LimitNum: 10 Milligram
  • Plant of Origin: Chinese herbal medicine
  • Testing Method: NMR/MS/HPLC
  • Product Ecification: 1mg-1kg
  • Heavy Metal: <10ppm
  • Voluntary Standards: company standard
  • Storage: Store in dry, dark and ventilated plac...
  • PackAge: Brown vial HDPE plastic bottle

Superiority

Hubei CuiRan Biotechnology Co., Ltd is a leading company in the research, development, manufacture and marketing of High Quality Phytochemicals and Extracts(especially Active Ingredients from Traditional Chinese Medicine,Traditional Chinese Medicine), Natural Active Pharmaceutical Ingredients worldwide. From small quantities for R&D or reference standard, to large quantities for customizing or manufacturing, Biopurify emphasizes on consistent and reliable services for his customers. 
With excellent quality products and good service, we have clients from more than dozens countries and regions, and we pride ourselves in providing our customers with a total satisfaction experiences.
We are doing our best to be your reliable partner for high quality Phytochemicals and Reference Standards from china.
 
Our main services:
A. Supply active ingredients and reference standards ofTraditional Chinese Medicine, from mgs to kgs scale.
B. Custom extraction and purification, target Herb Active Ingredients
C. Custom synthesis and semi-synthesis for Natural Active Ingredients
D. CR, CM and PD services from lab scale, pilot scale to commercial scale(GMP is also available)
E.Traditional Chinese Medicine compounds library
 

1.Provide traditional Chinese medicine reference materials and natural active ingredients;
2.More than 2200 compounds are available for selection, continuously building high-quality natural product libraries for drug research and development;
3.Provide various screening libraries and more inhibitor products;
4.Provide separation and structural determination of natural products;
5.Laboratory scale pilot to commercial scale collaborative research and process development services.More than 180 experiences in phytochemistry (still increasing)
Each product has passed very strict testing (NMR/MS/HPLC)
Agents from many countries

General tips:For obtaining a higher solubility , please warm the tube at 37 ℃ and shake it in the ultrasonic bath for a while.Stock solution can be stored below -20℃ for several months.
We recommend that you prepare and use the solution on the same day. However, if the test schedule requires, the stock solutions can be prepared in advance, and the stock solution must be sealed and stored below -20℃. In general, the stock solution can be kept for several months.
Before use, we recommend that you leave the vial at room temperature for at least an hour before opening it.
About Packaging:1. The packaging of the product may be reversed during transportation, cause the high purity compounds to adhere to the neck or cap of the vial.Take the vail out of its packaging and shake gently until the compounds fall to the bottom of the vial.
2. For liquid products, please centrifuge at 500xg to gather the liquid to the bottom of the vial.
3. Try to avoid loss or contamination during the experiment.
Shipping Condition:Packaging according to customer requirements(5mg, 10mg, 20mg and more). Ship via FedEx, DHL, UPS, EMS or other couriers with RT, or blue ice upon request.

Details

Chemical Properties of (-)-Syringaresnol-4-O-beta-D-apiofuranosyl-(1->2)-beta-D-glucopyranoside

Cas No. 136997-64-3    
PubChem ID 75412549 Appearance Powder
Formula C33H44O17 M.Wt 712.69
Type of Compound Lignans Storage Desiccate at -20°C
Solubility DMSO : 250 mg/mL (350.78 mM; Need ultrasonic)
Chemical Name (2S,3R,4S,5R,6R)-2-[4-[(3R,3aS,6R,6aS)-3-(4-hydroxy-3,5-dimethoxyphenyl)-1,3,3a,4,6,6a-hexahydrofuro[3,4-c]furan-6-yl]-2,6-dimethoxyphenoxy]-4-[(2S,3R,4R)-3,4-dihydroxy-4-(hydroxymethyl)oxolan-2-yl]oxy-6-(hydroxymethyl)oxane-3,5-diol
SMILES COC1=CC(=CC(=C1O)OC)C2C3COC(C3CO2)C4=CC(=C(C(=C4)OC)OC5C(C(C(C(O5)CO)O)OC6C(C(CO6)(CO)O)O)O)OC
Standard InChIKey RRKNBLZWFVIWPC-RKEBKKKYSA-N
Standard InChI InChI=1S/C33H44O17/c1-41-18-5-14(6-19(42-2)23(18)36)26-16-10-46-27(17(16)11-45-26)15-7-20(43-3)28(21(8-15)44-4)49-31-25(38)29(24(37)22(9-34)48-31)50-32-30(39)33(40,12-35)13-47-32/h5-8,16-17,22,24-27,29-32,34-40H,9-13H2,1-4H3/t16-,17-,22-,24-,25-,26+,27+,29+,30+,31+,32+,33-/m1/s1
General tips For obtaining a higher solubility , please warm the tube at 37 ℃ and shake it in the ultrasonic bath for a while.Stock solution can be stored below -20℃ for several months.
We recommend that you prepare and use the solution on the same day. However, if the test schedule requires, the stock solutions can be prepared in advance, and the stock solution must be sealed and stored below -20℃. In general, the stock solution can be kept for several months.
Before use, we recommend that you leave the vial at room temperature for at least an hour before opening it.
About Packaging 1. The packaging of the product may be reversed during transportation, cause the high purity compounds to adhere to the neck or cap of the vial.Take the vail out of its packaging and shake gently until the compounds fall to the bottom of the vial.
2. For liquid products, please centrifuge at 500xg to gather the liquid to the bottom of the vial.
3. Try to avoid loss or contamination during the experiment.
Shipping Condition Packaging according to customer requirements(5mg, 10mg, 20mg and more). Ship via FedEx, DHL, UPS, EMS or other couriers with RT, or blue ice upon request.

Source of (-)-Syringaresnol-4-O-beta-D-apiofuranosyl-(1->2)-beta-D-glucopyranoside

From Albizia julibrissin Duraz.

Biological Activity of (-)-Syringaresnol-4-O-beta-D-apiofuranosyl-(1->2)-beta-D-glucopyranoside

Description (-)-Syringaresnol-4-O-beta-D-apiofuranosyl-(1->2)-beta-D-glucopyranoside is a natural lignan from Albizia julibrissin Durazz..

Protocol of (-)-Syringaresnol-4-O-beta-D-apiofuranosyl-(1->2)-beta-D-glucopyranoside

Structure Identification

Beijing Da Xue Xue Bao. 2003 Apr 18;35(2):180-3.

Isolation and identification of chemical constituents from Albizia julibrissin Durazz..[Pubmed: 12920839]

To study the chemical constituents of the stem bark of Albizia julibrissin Duraz..
METHODS AND RESULTS:
Chemical constituents were isolated and their structures identified by the repeated chromatography and spectral analysis. Five compounds were obtained as follows: (-)-Syringaresnol-4-O-beta-D-apiofuranosyl-(1->2)-beta-D-glucopyranoside (1), (6R)-trans-2,6-dimethyl-6-O-beta-D-quinovosyl-2,7-menthiafolic acid (2), (6S)-trans-2,6-dimethyl-6-O-beta-quinovosyl-2,7-menthiafolic acid (3), 5,5'-dimethoxy-7-oxolariciressinol (4) and (-)syringaresinol (5).
CONCLUSIONS:
Compounds 2, 3 and 4 were new natural products isolated from this plant for the first time.

Preparing Stock Solutions of (-)-Syringaresnol-4-O-beta-D-apiofuranosyl-(1->2)-beta-D-glucopyranoside

  1 mg 5 mg 10 mg 20 mg 25 mg
1 mM 1.4031 mL 7.0157 mL 14.0313 mL 28.0627 mL 35.0784 mL
5 mM 0.2806 mL 1.4031 mL 2.8063 mL 5.6125 mL 7.0157 mL
10 mM 0.1403 mL 0.7016 mL 1.4031 mL 2.8063 mL 3.5078 mL
50 mM 0.0281 mL 0.1403 mL 0.2806 mL 0.5613 mL 0.7016 mL
100 mM 0.014 mL 0.0702 mL 0.1403 mL 0.2806 mL 0.3508 mL
* Note: If you are in the process of experiment, it's necessary to make the dilution ratios of the samples. The dilution data above is only for reference. Normally, it's can get a better solubility within lower of Concentrations.

References on (-)-Syringaresnol-4-O-beta-D-apiofuranosyl-(1->2)-beta-D-glucopyranoside

[Isolation and identification of chemical constituents from Albizia julibrissin Durazz.].[Pubmed:12920839]

Beijing Da Xue Xue Bao Yi Xue Ban. 2003 Apr 18;35(2):180-3.

OBJECTIVE: To study the chemical constituents of the stem bark of Albizia julibrissin Duraz.. METHODS: Chemical constituents were isolated and their structures identified by the repeated chromatography and spectral analysis. RESULTS: Five compounds were obtained as follows: (-)-Syringaresnol-4-O-beta-D-apiofuranosyl-(1-->2)-beta-D- glucopyranoside (1), (6R)-trans-2,6-dimethyl-6-O-beta-D-quinovosyl-2,7-menthiafolic acid (2), (6S)-trans-2,6-dimethyl-6-O-beta-quinovosyl-2,7-menthiafolic acid (3), 5,5'-dimethoxy-7-oxolariciressinol (4) and (-)syringaresinol (5). CONCLUSION: Compounds 2, 3 and 4 were new natural products isolated from this plant for the first time.

Description

(-)-Syringaresnol-4-O-β-D-apiofuranosyl-(1→2)-β-D-glucopyranoside is isolated from the bark of Albizzia myriophylla.

Keywords:

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